IKA RV 10 basic Operating Instructions Manual

Text of IKA RV 10 basic User Guide:

• IKA RV 10 basic, IKA®RV 10 basic IKA®RV 10 digital 042009 Betriebsanleitung DE 5 Operating instructions EN 17 Mode d’emploi FR 29 Instrucciones de manejo ES 41 36 785 00 Reg.-No. 4343-01 3678500_RV10bd_032009_4sprachig_ue:Layout 1 22.07.2009 17:30 Uhr Seite 1

• IKA RV 10 basic, 042009 17 Interfaces and outputs 22 Commissioning 23 Maintenance and cleaning 24 Accessories 25 Error codes 27 Technical data 27 Solvent table (excerpt) 28 Warranty 28 • Use the HB 10.2 cover or the HB 10.1 spray guard. • Only use the device under an all side-closed exhaust, or a com- pa rable protective device. • Adapt the quantity and the type of distilland to the size of the di- stillation equipment. The cooler must work properly. Monitor the coolant flow rate at the cooler outlet. • The glass equipment must always be ventilated when working under normal pressure (e.g. open outlet at

• IKA RV 10 basic, • The device is only disconnected from the power supply network if the device power switch is off or the plug is pulled out. • The socket for the mains cord must be easily accessible. • Use  Together with the accessories recommended by IKA, the device is suitable for: - quick and gentle distillation of liquids - evaporation of solutions and suspensions - crystallisation, synthesis or cleaning of fine chemicals - drying of powder and granulate material - recycling of solvents Mode of operation: Tabletop device • Range of use - Laboratories - Schools -

• IKA RV 10 basic, 042009 19 Drive RV 10 basic/digital CAUTION! Loosen transportation lock (fig. 4a)! ☞ Hold the lift with your hand on the height position and remove the thumb screw on the back of the appliance (A). ☞ Once the transportation lock has been removed, the lift moves slowly to its upper end position. The distance is approx. 140 mm. ☞ Connect the device to the power supply (B) using the supplied power cord (B). Adjustable base (Fig. 4b) ☞ Attach the bracket for the Woulff bottle to the left side of the lift (fig. 5). ☞ Insert the bottle and attach the supplied hose connectors to the bottle (fig. 6). ☞ Remove the clam

• ☞ Feed the steam pipe in until it stops. ☞ Then lock the locking device by turning it clockwise by 60° (fig. 10). ☞ Check the axial locking device on the steam pipe. Push-off mechanism The plastic screw nut (E) helps loosen tight-fitting piston ground-in connections (Fig. 10). ☞ The plastic screw nut (E) helps loosen tight-fitting piston ground- in connections (Fig. 10). ☞ To do

• IKA RV 10 basic, Removing the condenser ☞ Use the ring spanner provided to loosen union nuts that are tightly fitted. ☞ Loosen the union nut by turning anticlockwise. Description of special condensers • RV10.3 Vertical-intensive condenser with manifold This vertical-intensive condenser features a double jacket design for particularly efficient condensation. Also available with coating (RV10.30) • RV10.4 Dry ice condenser Dry ice condenser for distilling low-boiling solvents. Cooling by dry ice, no cooling water required. Maximum conden- sation thanks to low temperatures. Also

• IKA RV 10 basic, Data transfer HB 10 digital The heating bath transfers data via IR interfaces. These are located on the left display side of the heating bath or on the right side of the drive unit. Do not place any objects between the two operating units as otherwise the data transfer may be interrupted (fig. 15)! RV10 digital The RS 232 interface at the back of the device is fitted with a 9-pole SUB-D jack and can be connected to a PC. The pins have serial si- gnals. Using the laboratory device software “labworldsoft”, the de- vice can be operated in “Remote” mode. Note: Please note the sy

• IKA RV 10 basic, 042009 23 ☞ Set the target value “Int” on the knob by turning (1 to 60 minu- tes). ☞ Starting the “Int” function - Automatic when rotation drive is running - Start the rotation drive Note: In interval mode the maximum speed is limited to 200 rpm. ☞ Save the “Int” target value by pressing the "Int" key again. ☞ Deactivate the interval by setting the target value to “0”. Display (see page 4) • Display “REMOTE” (10) (only for RV 10 digital) Remote control via PC in connection with software “labworldsoft” is active. • Display “888 rpm” (20) Current target and actual speed indicator in rev

• Setting up the heating bath Refer also to the operating instructions for the HB 10 basic /di- gital heating bath! ☞ Move the lift to the bottom position and check the position of the heating bath in relation to the evaporator piston. When using lar- ger evaporator pistons (2 or 3 litres) or depending on the angle of the rotation drive, you can move the heating bath 50 mm to the right. ☞ F

• IKA RV 10 basic, Accessories RV 10.1 NS 29/32 Vertical glassware (1) RV 10.10 NS 29/32 Vertical glassware, coated (1) RV 10.2 NS 29/32 Diagonal glassware (2) RV 10.20 NS 29/32 Diagonal glassware, coated (2) RV 10.700 NS 29/42 Vertical glassware (1) RV 10.710 NS 29/42 Vertical glassware, coated (1) RV 10.800 NS 29/42 Diagonal glassware (2) RV 10.810 NS 29/42 Diagonal glassware, coated (2) RV 10.900 NS 24/40 Vertical glassware (1) RV 10.910 NS 24/40 Vertical glassware, coated (1) RV 10.1000 NS 24/40 Diagonal glassware (2) RV 10.1010 NS 24/40 Diagonal glassware, coated (2) RV 10.3 Vertical-intensive condenser with manifold RV 10.30 Vertical-intensive condenser with manifold, coated RV 10.4 Dry

• IKA RV 10 basic, 042009 26 RV 10.200 KS 35/20 Receiving flask, coated 100 ml RV 10.201 KS 35/20 Receiving flask, coated 250 m RV 10.202 KS 35/20 Receiving flask, coated 500 ml RV 10.203 KS 35/20 Receiving flask, coated 1000 ml RV 10.204 KS 35/20 Receiving flask, coated 2000 ml RV 10.205 KS 35/20 Receiving flask, coated 3000 ml RV10.300 NS 29/32 Powder piston 500 ml RV10.301 NS 29/32 Powder piston 1000 ml RV10.302 NS 29/32 Powder piston 2000 ml RV10.303 NS 24/29 Powder piston 500 ml RV10.304 NS 24/29 Powder piston 1000 ml RV10.30

• Error codes Any malfunctions during operation will be identified by an error message on the display (only for RV 10 digital). Once a serious error message has been displayed, the lift moves to the top end position and the device can no longer be operated. The lift can be operated again. Proceed as follows in such cases: ☞ Switch off device using the main switch (A) ☞ Carry out corrective m

• IKA RV 10 basic, 28 042009 Solvent Formula Pressure for boiling point 40 °C in mbar Acetic acid C 2 H 4 O 2 44 Acetone C 3 H 6 O 556 Acetonitrile C2H3N 226 N-Amylalcohol, C 5 H 12 O11 n-Pentanol n-Butanol C 4 H 10 25 tert. Butanol, C 4 H 10 O 130 2-Methyl-2-Propanol Butylacetate C 6 H 12 O 2 39 Chlorobenzene C 6 H 5 CI 36 Chloroform CHCI 3 474 Cyclohexane C 6 H 12 235 Dichloromethane, CH 2 CI 2 atm.press. Methylenechloride Diethylether C 4 H 10 O atm.press. 1,2,-Dichloroethylene (trans) C 2 H 2 CI 2 751 Diisopropylether C 6 H 14 O 375 Diox

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