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Philips PC-APD PW-1710 Operation & User’s Manual

  • PC-APD PW-1710 Portable Generator
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Philips PC-APD PW-1710 Manual Online:

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Philips PC-APD PW-1710 User Manual
Philips PC-APD PW-1710 User Guide
Philips PC-APD PW-1710 Online Manual

Text of Philips PC-APD PW-1710 User Guide:

  • Philips PC-APD PW-1710, LABORATORY MANUAL AND INSTRUCTIONS Version 1.3 Metallurgical & Materials Engineering Dr. M.L. Weaver W.S. Rollings September 6, 2000 This manual describes operation of the Philips PW-1710 X-ray generator using PC-APD, techniques for data collection and analysis, and for instrument shutdown. All users should refer to the proper manuals for detailed information. IMPORTANT! DO NOT STORE YOUR DATA ON THE C: OR D: DRIVE OF THE COMPUTER. THE

  • Philips PC-APD PW-1710, INSTRUCTIONS FOR PHILIPS X-RAY GENERATOR TURNING ON THE X-RAY GENERATOR 1) SIGN THE LOG SHEET! 2) Turn on the water chiller and wait 1 minute. The water pressure should be ≥ 40 psi. 3) On the x-ray generator, set the voltage and current to the lowest available setting (i.e., turn the kV and mA knobs all of the way to the left). 4) Turn on the x-ray generator by depressing the [ON] button on the display console (see Fig A). 5) Press the start button and then wait for the yellow “X-ray On” light to illuminate. This will occur approximately 30 seconds after you depress the button. 6) Wait 1 minute. Turn voltage up to 25 kV. 7) Wait 15 minutes. Gra

  • Philips PC-APD PW-1710, 10) On the small shutter control panel (Figure C), select window 2. Open the shutter by turning the selector knob to ∞ (one click to the right). Press the red ON button. The yellow light for shutter 2 will come on. 11) The instrument is now ready to collect data. Setup your data collection program in PC-APD and run it. SEE THE NOTES FOR PC-APD ON THE ACCOMPANYING PAGES. 12) Turn on the computer. In the Windows 3.1 environment, open the Philips folder and double click the “XMENU” icon. 13) Select “PC-APD” from the men

  • Philips PC-APD PW-1710, 25) Alter the field to collect a standard powder measurement. See Figure 3. 26) Press [Esc] twice to return to the main APD menu. 27) Choose DATA COLLECTION (D). 28) Choose IDENTIFY MEASUREMENT (I). 29) Enter the name of the identify program that was just created. Press [Enter]. Press F5 to see a list of available identify programs if necessary. 30) Enter the sample identification and a filename where the data will be stored in the appropriate fields. 31) Check for the following:  Sample should be on the stage  Instrument door should be closed.  Power should

  • S Y S T E M P A R A M E T E R S 6-Sep-00 13:12:32 Licensee: Some Laboratory Tuscaloosa, AL Identification: Philips Analytical PC-APB, Diffraction software Data directory: C:\APD\DATA Temporary files: C:\APD\TMP Graphics Adapter: VGA Graphics hard copy device: PRINTER Monitor: COLOUR Number of pens: Serial port Used for Baudrat

  • Philips PC-APD PW-1710, PARAMETERS FOR PW3710 BASED DIFFRACTOMETER 6-Sep-00 13:12:32 Sample Changer: NO Spinner: NO Tube Anode: Cu Focus: NF (Normal Focus) Programmable generator (PW1825): NO Generator tension [kV]: 45 Generator current [mA]: 40 Divergence slit: 1/12° Separate θ drive: NO Receiving Slit [mm]: 0.2 Monochromator: YES Lower level [%]: 30 Upper level [%]: 80 Maximum 2 θ [°]: 120.000 Temperature control unit: NONE Esc=Last menu F1=Save current settings F10=Help FIGURE 2. Schematic of SYSTEM PARAMETERS menu.

  • I D E N T I F Y : S C A N P A R A M E T E R S 6-Sep-00 13:12:32 New program: Type of Program: CONTINUOUS Step size [°2 θ ]: 0.020 Start Angle [°2 θ ]: 10.000 Maximum d-value [Å]: 8.83820 End Angle [°2 θ ]: 70.000 Minimum d-value [Å]: 1.34298 Scan time [h:m:s]: 0:50:00 Number of steps: 3000 Time per step [s]:

  • Philips PC-APD PW-1710, ANALYZING DATA ANALYZING DATAANALYZING DATA ANALYZING DATA The following procedures explain the use of the APD and IDENTIFY software to analyze collected data. Patterns must be treated using the APD software prior to identification using the IDENTIFY sofware. 1. Choose APD from X-MENU and from the main menu select PATTERN TREATMENT (P). 2. Choose ALPHA 2 STRIPPING (A). The patterns contained in the ICDD do not contain alpha 2 peaks, so in order to achieve the most accurate match these peaks should be removed from the collected data. If you do not want to remove the alpha 2 peaks from the collected data then proce

  • Philips PC-APD PW-1710, P E A K S E A R C H 6-Sep-00 13:12:32 Input file: HDPE .RD DI file: HDPE .DI Create background file: NO Create peak data file: NO Creeate smoothed data file: NO Create second derivative file: NO Start angle [°2 θ ]: 0.200 End angle [°2 θ ]: 0.260 Minimum peak tip width [°2 θ ]: 0.04 Maximum peak tip width [°2 θ ]: 1.00 Peak base width [°2 θ ]: 2.00 Minimum significance: 0.75 Converty fixed slit intensities to automatic slit inten

  • Philips PC-APD PW-1710, 17. Enter the name of the DI file (this file was created when the peak search was performed and has the same name as the raw data file but a DI extension) to be edited. 18. Press F1 to edit the lines. 19. Peaks can be added, deleted or moved. To add a peak press F4 for insert and then F8 for graphical mode. Then, position the cursor on the tip of the peak to be added and press F1 to accept the peak position. To delete a peak, use the F1 and F2 keys to page through the listing of peaks. Then use the arrow keys to highlight the 2 theta value of the peak to be deleted. Press F3 t

  • Philips PC-APD PW-1710, 23. You will be brought to the PC-Identify main window (Figure 3). Figure 3. PC-Identify main window. 24. Choose IDENTIFY (I) and press F1 or ENTER. You will be prompted with a highlighted entry box as indicated in Figure 4.

  • Philips PC-APD PW-1710, Figure 4 25. Select the appropriate data directory and press ENTER. 26. Enter the name of the desired DI file or press F5 to select from a list of available DI files. 27. Press F1 to continue with analysis. You will be prompted with the following screen:

  • Philips PC-APD PW-1710, Figure 5 28. Use the ‘+’ or ‘-‘ keys to toggle the parameters setting to ‘Normal’, ‘Precise’ or ‘User defined’ depending upon the type of analysis that you want to do.  A ‘Normal’ setting is appropriate for general analysis.  The ‘User defined’ option can be used to limit the scope of your search to select ICDD cards or to compounds containing selected elements.  Refer to the PC-IDENTIFY Users Manual for more details. 29. Press F1 to start the analysis. 30. The entire ICDD/JCPDS databa

  • Philips PC-APD PW-1710, 32. The list of patterns can now be compared to both the DI file and the raw data file. Pressing the ‘+’ and ‘-‘ keys steps through the list of candidates and pressing F4 and F3 insert and delete the reference patterns from the raw data field.

  • Philips PC-APD PW-1710, TURNING OFF THE X-RAY GENERATOR 1. Close the shutter by turning the appropriate knob on the Shutter Control Box (Figure C) to off. Lower the current to the lowest mA by turning the mA knob all of the way to the left. Reduce the voltage to 25 kV. WAIT 5 MINUTES. 2. Lower the voltage to 10 kV (i.e., lowest kV). 3. Turn off the X-ray generator by pressing the [STOP] button. Turn off the power by pressing the [OFF] button. 4. Feel the top of the x-ray tube, when it is cool the water chiller may be turned off. 5. Data analysis and manipulation may be performe

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